China 75932-02-4 N-α,N-ε-di-Fmoc-D-lysine Onye nrụpụta na ụlọ ọrụ |Jiayinglai

75932-02-4 N-α,N-ε-di-Fmoc-D-lysine

Nkọwa dị mkpirikpi:

Ọdịdị	Na-acha ọcha na-acha ọcha ntụ ntụ
MF	C36H34N2O6
MW	590.66
Ịdị ọcha	98+

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Nkọwa ngwaahịa

Ọnọdụ njem&ụkpụrụ mbupu akwadoro:
site n'ikuku, site n'oké osimiri ma ọ bụ site na awara awara

Ọnọdụ nchekwa:
2-8 Celsius C

Ọnụ ahịa kacha nta:
Mkparịta ụka

Asambodo:
COA, HPLC, GC, HNMR, Assay, Ọdịnaya Mmiri (KF), TLC dị

Ụdị okwu

Na,Ne-di-Fmoc-D-lysine;

N-.ALPHA.,N-.EPSILON.-DI-FMOC-D-LYSINE;

(R) -1,13-di (9H-fluoren-9-yl) -3,11-dioxo-2,12-dioxa-4,10-diazatridecane-5-carboxylicacid;

D-Lysine, N2, N6-bis[(9H-fluoren-9-ylMethoxy) carbonyl]-;

FMoc-D-Lys(FMoc)-OHN-α,N-ε-di-FMoc-D-lysine;

N2,N6-Bis-FMoc-D-lysine;

N2,N6-Bis[(9H-fluoren-9-ylMethoxy)carbonyl]lysine

Nkwakọ ngwaahịa n'ime

A na-ejikarị ha ebu ntụ ntụ.Ha nwekwara ike igbochi anwụ na mmiri ime ihe ọjọọ.

mpụta mbukota

Katọn ahụ siri ike nwere ike ichekwa ngwaahịa gị ka ọ ghara ịdaba na mmiri.

Ngwa

Amino acid na-echebe ugboro abụọ na-agụnyekarị D-lys-OH nwere otu amino dị iche iche nwere yinye akụkụ yana yinye nwere akụkụ.pMgbanwe nke L-Rag-OH.Maka otu AA-amin, a ka na-anabata atụmatụ nchekwa FMOC, na nwanne nna nke abụọ nke carbonate abụọ na-eji n'akụkụ akụkụ.A na-ewebata Tibon n'ime otu ikuku oxygenyl iji chebe Fu Fu 5 ~ Sulfidal iji chebe.N'ihi na enwere ọtụtụ usoro njikọ maka amino acid abụọ a, nzaghachi bụ isi na nzaghachi bụ isisteps na-eme nnwale njikarịcha otu ihe.Nchedo nke D-LYS-OH na-atụlekarị oge na-emetụta ọgbọ nke ọla kọpa dabarankeokpomọkụ, na oge iji wepụ ọla kọpa.Nchedo nke L-Rag-OH tumadi na-atụle nkwadebe nke Z-RG-OH. N'oge ahụ, okpomọkụ nke ZL-Rag (PBF) -OH mgbanaka nke amonia nnu, yana ọnụ ọgụgụ nke ihe na-akpata mgbe hydrogen na-agbanye na Z,

Nrụgide, okpomọkụ na oge mmeghachi omume ahụ enwetala nsonaazụ dị mma site na nyocha kachasị mma.

N'oge usoro mmeghachi omume, a na-anabata usoro mmeghachi omume nchọpụta TL.C, yana ọnọdụ kristal nke ngwaahịa ahụ ka kachasị.

A na-atụle ịdị ọcha nke ngwaahịa ahụ site na chromatography mmiri na-arụ ọrụ dị elu, na ịdị ọcha nke ngwaahịa ahụ ruru ihe karịrị 95.0%.Na mgbakwunye na ihe ịrịba ama anụ ahụ mgbe niile, kwaincluding infrared spectrum, mass spectrum ma ọ bụ hydrogen spectrum.

ngwaahịa ndị metụtara ya

L-Lys (Boc)	Lys (Fmoc) - OH	L-Lys(Cbz)-OH	D-Lys (Fmoc) .HCl
Lys (Fmoc) .HCl	Boc-Lys (Boc) - OH	Boc-L-Lys(Boc)-OH·DCHA	Boc-D-Lys(Boc)-OH
Boc-L-Lys(Fmoc) -OH	Fmoc-L-Lys(tfa) -OH	Fmoc-L-Lys (DDC)	Fmoc-L-Lys (Cbz)
Fmoc-L-Lys(AC)	Fmoc-L-Lys(Fmoc) -OH	Fmoc-D-Lys(Boc) -OH	Fmoc-L-Lys(Boc) -OH
Cbz-L-Lys(Fmoc) -OH	Z-DL-Lys(cbz)-OH
Fmoc-Gly-Ol	Gly-Gly-Leu	H-Gly-Obzl.Tos	Boc-Trp-Gly
Fmoc-Gly-OH	Gly-Gly-Gly	Gly-Obzl	Fmoc-L-Thr(tBu) -Gly-OH
Fmoc-Gly-Val-OH	Ala-gly	Gly-Obzl.hcl	Met-Gly.HCl
Fmoc-Gly-Gly-OH	Ala-Gly-Ome.hcl	Tos-Gly-Ome	H-Met-Gly-OH
Fmoc-Gly-Gly-Gly-OH	Boc-Ala-Gly-OH	H-Gly-Oet.HCl	Cbz-D-Arg-Gly-OH
Fmoc-Gly-Gly-Gly-Gly-OH	Fmoc-Ala-gly-OH	Gly.HCL	Boc-His(Trt)-Gly-OH
H-Gly-NH2.HCl	Boc-Gly-OL

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