China 122235-70-5 BOC-DAP (FMOC) -OH Onye nrụpụta na ụlọ ọrụ |Jiayinglai

122235-70-5 BOC-DAP(FMOC) -OH

Nkọwa dị mkpirikpi:

Ọdịdị	Ọcha ka Gbanyụọ-Ọcha ntụ ntụ
MF	C23H26N2O6
MW	426.46
Ịdị ọcha	98+

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Nkọwa ngwaahịa

Ọnọdụ njem&ụkpụrụ mbupu akwadoro:
site n'ikuku, site n'oké osimiri ma ọ bụ site na awara awara

Ọnọdụ nchekwa:
2-8 Celsius C

Ọnụ ahịa kacha nta:
Mkparịta ụka

Asambodo:
COA, HPLC, GC, HNMR, Assay, Ọdịnaya Mmiri (KF), TLC dị

Ụdị okwu

Boc-3- (Fmoc-amino) -L-alanine, Nα-Boc-Nβ-Fmoc-L-2,3-diaminopropionicacid;

NALPHA-tert-Butoxycarbonyl-NB-9-fluorenylmethoxycarbonyl-L-2,3-diaminopropi;

N-.ALPHA.-BOC-N-.BETA.-FMOC-L-2,3-DIAMIOPROPIONICACID;

N-Boc-N-Fmoc-(S)-2,3-diaminopropionicacid;

N-a-Boc-N-β-Fmoc-L-2,3-diamiopropionicacid;

(S) -2,3-Diaminopropanoicacid, N2-BOC,N3-FMOC echedoro;

3-[(9H-Fluoren-9-ylmethoxycarbonyl) amino] -L-alanine, N-BOC echedoro;

Boc-Dapa(FMoc) -OH

Nkwakọ ngwaahịa n'ime

A na-ejikarị ha ebu ntụ ntụ.Ha nwekwara ike igbochi anwụ na mmiri ime ihe ọjọọ.

mpụta mbukota

Katọn ahụ siri ike nwere ike ichekwa ngwaahịa gị ka ọ ghara ịdaba na mmiri.

Ngwa

Amino acid na-echebe ugboro abụọ na-agụnyekarị D-lys-OH nwere otu amino dị iche iche nwere yinye akụkụ yana yinye nwere akụkụ.pMgbanwe nke L-Rag-OH.Maka otu AA-amin, a ka na-anabata atụmatụ nchekwa FMOC, na nwanne nna nke abụọ nke carbonate abụọ na-eji n'akụkụ akụkụ.A na-ewebata Tibon n'ime otu ikuku oxygenyl iji chebe Fu Fu 5 ~ Sulfidal iji chebe.N'ihi na enwere ọtụtụ usoro njikọ maka amino acid abụọ a, nzaghachi bụ isi na nzaghachi bụ isisteps na-eme nnwale njikarịcha otu ihe.Nchedo nke D-LYS-OH na-atụlekarị oge na-emetụta ọgbọ nke ọla kọpa dabarankeokpomọkụ, na oge iji wepụ ọla kọpa.Nchedo nke L-Rag-OH tumadi na-atụle nkwadebe nke Z-RG-OH. N'oge ahụ, okpomọkụ nke ZL-Rag (PBF) -OH mgbanaka nke amonia nnu, yana ọnụ ọgụgụ nke ihe na-akpata mgbe hydrogen na-agbanye na Z,tya nrụgide, okpomọkụ na oge nke mmeghachi omume enwetawo ezigbo mmepụta site na njikarịcha nnwale.

N'oge usoro mmeghachi omume, a na-anabata usoro mmeghachi omume nchọpụta TL.C, yana ọnọdụ kristal nke ngwaahịa ahụ ka kachasị.

A na-atụle ịdị ọcha nke ngwaahịa ahụ site na chromatography mmiri na-arụ ọrụ dị elu, na ịdị ọcha nke ngwaahịa ahụ ruru ihe karịrị 95.0%.Na mgbakwunye na ihe ịrịba ama anụ ahụ mgbe niile, kwaincluding infrared spectrum, mass spectrum ma ọ bụ hydrogen spectrum.

ngwaahịa ndị metụtara ya

Boc-D-Dap(Boc).DCHA	Boc-Dap(Boc)-OH.DCHA	Boc-D-Dap(Fmoc) -OH	Boc-Dap(Cbz) -OH
Boc-D-Dap(Cbz)-OH	Fmoc-L-Dap(Fmoc) -OH	Fmoc-L-Dap(Cbz) -OH	Fmoc-D-Dap(cbz)
Cbz-D-Dap(BOC)-OH	Cbz-L-Dap(Fmoc) -OH

Nke kacha elu

1. R&D ọrụ dị
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